Effect of Prior Martensite on Mechanical Properties of Austempered Ductile Iron

Effect of Prior Martensite on Mechanical Properties of Austempered Ductile Iron

Chen Yang Derek O. Northwood Cheng Liu

College of Mechanical Engineering, Yangzhou University, PR China

Department of Mechanical, Automotive and Materials Engineering, University of Windsor, Canada

Page: 
455-462
|
DOI: 
https://doi.org/10.2495/CMEM-V6-N3-455-462
Received: 
N/A
| |
Accepted: 
N/A
| | Citation

OPEN ACCESS

Abstract: 

An unalloyed ductile iron, which incorporates C and Si as major and Mn as minor alloying elements, is processed by a novel austempering process, in order to obtain superior mechanical properties. The samples are initially austenitized at 890°C for 20 min, then quenched into patented water-based quenching liquid at 180°C for 0.5, 2 and 3.5 s respectively, and austempered at 220°C for 240 min in an electric furnace. Optical microscopy (OM) and scanning electron microscopy (SEM) are performed to correlate the mechanical properties with microstructural characteristics. It is found that partial martensite can be formed firstly upon quenching, which will accelerate the subsequent bainitic transformation and promote refinement of multiphase colonies during austempering. The prior martensite content increases with increasing holding time during quenching. A tensile strength of 1330MPa, an elongation of 3.13% and a hardness of 45HRC can be achieved by controlling the prior martensite content to 12%. SEM of fracture surfaces reveals a mixed ductile and cleavage rupture morphology type in all samples. The results indicate that the tensile behavior of the investigated ADI is mainly influenced by the content of prior martensite.

Keywords: 

austempering process, bainitic transformation, prior martensite, tensile strength

  References

[1] Harding, R.A., The production, properties and automotive applications of austempered ductile iron. Metals and Materials, 45(1), pp. 1–16, 2007.

[2] Zhang, N., Zhang, J.W., Lu, L.T., Zhang, M.T., Zeng, D.F. & Song, Q.P., Wear and friction behavior of austempered ductile iron as railway wheel material. Materials & Design, 89, pp. 815–822, 2015.https://doi.org/10.1016/j.matdes.2015.10.037

[3] Dong, J.L., Ju, F.C., Chen, H.S. & Chen, L.W., Influence of austempering temperature on fracture toughness in bainitic nodular cast iron. Journal of Materials Science Letters, 5(5), pp. 555–558, 1986.https://doi.org/10.1007/BF01728689

[4] Yang C., Cui, X.X., Zhao, Z.B., Hua, G. & Liu, C., Role of bulky retained austenite in austempered ductile iron. Advanced Materials Research, 1142, pp. 19–22, 2016. https://doi.org/10.4028/www.scientific.net/AMR.1142.19

[5] Garin, J.L. & Mannheim, R.L., Strain–induced martensite in ADI alloys. Journal of Materials Processing Technology, 143–144(1), pp. 347–351, 2003. https://doi.org/10.1016/S0924-0136(03)00452-7

[6] Panneerselvam, S., Martis, C.J., Putatunda, S.K. & Boileau, J.M., An investigation on the stability of austenite in austempered ductile cast iron (ADI). Materials Science & Engineering A, 626(7), pp. 237–246, 2015. https://doi.org/10.1016/j.msea.2014.12.038

[7] Sohi, M.H., Ahmadabadi, M.N. & Vahdat, A.B., The role of austempering parameters on the structure and mechanical properties of heavy section ADI. Journal of Materials Processing Technology, 153(1), pp. 203–208, 2004. https://doi.org/10.1016/j.jmatprotec.2004.04.308

[8] Ahmadabadi, M.N., Ghasemi, H.M. & Osia, M., Effects of successive austempering on the tribological behavior of ductile cast iron. Wear, 231(2), pp. 293–300, 1999. https://doi.org/10.1016/S0043-1648(99)00163-5

[9] Toktaş, G.M., Tayanç, M. & Toktaş, A., Effect of matrix structure on the impact properties of an alloyed ductile iron. Materials Characterization, 57(4–5), pp. 290–299, 2006. https://doi.org/10.1016/j.matchar.2006.02.008

[10] Hamid Ali, A.S. & Elliot, R., Austempering of a Mn–Mo–Cu alloyed ductile iron part1austempering kinetics and processing windows. Materials Science and Technology, 12(12), pp. 1021–1031, 1996.https://doi.org/10.1179/mst.1996.12.8.679

[11] Putatunda, S.K., Singh, I. & Bartosiewicz, L., Influence of chromium on mechani  cal properties of austempered ductile cast iron. Journal of Materials Engineering and Performance, 4(1), pp. 90–101, 1995.https://doi.org/10.1007/BF02682710

[12] Toktaş, G., Tayanç, M. & Toktaş, A., Effect of matrix structure on the impact properties of an alloyed ductile iron. Materials Characterization, 57(4–5), pp. 290–299, 2006. https://doi.org/10.1016/j.matchar.2006.02.008

[13] Mallia, J., Grech, M. & Smallman, R.E., Effect of silicon content on transformation kinetics of austempered ductile iron. Materials Science and Technology, 14(5), pp. 452–460, 1998.https://doi.org/10.1179/mst.1998.14.5.452

[14] Hsu, C.H. & Lin, K.T., A study on microstructure and toughness of copper alloyed and austempered ductile irons. Materials Science & Engineering A, 528(18), pp. 5706–5712, 2011.https://doi.org/10.1016/j.msea.2011.04.035

[15] Balos, S., Radisavljevic, I., Rajnovic, D., Tabakovic, S., Cekic, O.E. & Sidjanin, L., Geometry, mechanical and ballistic properties of ADI material perforated plates. Materials & Design, 83, pp. 66–74, 2015. https://doi.org/10.1016/j.matdes.2015.05.081

[16] Bayati, H. & Elliott, R., A stepped austempering heat treatment for a Mn alloyed ductile cast iron. Advanced Materials Research, 4–5, pp. 399–406, 1997. https://doi.org/10.4028/www.scientific.net/AMR.4-5.399

[17] Putatunda, S.K., Development of austempered ductile cast iron (ADI) with simultaneous high yield strength and fracture toughness by a novel two-step austempering process. Materials Science & Engineering A, 315(1), pp. 70–80, 2001. https://doi.org/10.1016/S0921-5093(01)01210-2

[18] Putatunda, S.K., Comparison of the mechanical properties of austempered ductile cast iron (ADI) processed by conventional and step-down austempering process. Materials and Manufacturing Processes, 25(8), pp. 749–757, 2010. https://doi.org/10.1080/10426910903367394

[19] Darwish, N. & Eliott R., Austempering of low manganese ductile irons part 3 variation of mechanical properties with heat treatment conditions. Materials Science and Technology, 9(10), pp. 572–585, 1993.https://doi.org/10.1179/mst.1993.9.10.882

[20] Liu, C., Yang, C., Cui, X.X., Zhao, Z.B. & Hua, G., Bending property of ductile cast iron by a novel austempering. Transactions of Materials and Heat Treatment, 37, pp. 22–25, 2016. (In Chinese)

[21] Liu, C., Zhao, Z.B. & Bhole, S.D., Lathlike upper bainite in a silicon steel. Materials Science & Engineering A, 434(1–2), pp. 289–293, 2006. https://doi.org/10.1016/j.msea.2006.06.078

[22] Gong, W., Tomota, Y., Harjo, S., Sua, Y.H. & Aizawaa, K., Effect of prior martensite on bainite transformation in nanobainite steel. Acta Materialia, 85, pp. 243–249, 2015. https://doi.org/10.1016/j.actamat.2014.11.029

[23] Stokes B., Gao, N. & Reed, P.A.S., Effect of graphite nodules on crack growth behavior of austempered ductile iron. Materials Science and Engineering A, 445–446(6), pp. 374–385, 2007.https://doi.org/10.1016/j.msea.2006.09.058