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Synthesis and Characterization of Li(Li0.05Ni0.6Fe0.1Mn0.25)O2 Cathode Material for Lithim Ion Batteries

Centre for Scientific and Applied Research, PSN College of Engineering and Technology, Tirunelveli-627 152, Tamil Nadu, India.

St. Mother Theresa Engineering College, Vagaikulam, Mudivaithanenthal Post, Thoothukudi, Tamil Nadu 628 102, India

Department of Physics, Saveetha School of Engineering, Saveetha University, Thandalam – 602105, Chennai, Tamil Nadu, India.

Division of Electronics and Electrical Engineering, Dongguk University-Seoul, Seoul 04620, South Korea

K.Ramakrishnan College of Technology, Samayapuram, Trichy-621 112

Department of Physics, Alagappa University, Karaikudi 630 003, Tamil Nadu, India

Facultad de Ingeniería, UABC Mexicali, 21280, México

Corresponding Author Email:

sthanikai@rediffmail.com, shajan89@gmail.com

Received:

31 October 2017

| |

Accepted:

22 January 2018

| | Citation

v21n01a09_p051-056.pdf

OPEN ACCESS

Abstract:

A new type of lithium enriched cathode material Li (Li_0.05Ni_0.6Fe_0.1Mn_0.25)O₂ was synthesized by sol-gel method with citric acid as a chelating agent. The structural and morphological studies were systematically investigated through X-ray diffraction, SEM with EDS, FT-IR and Raman analyses. The crystallite size of the Li (Li_0.05Ni_0.6Fe_0.1Mn_0.25)O₂cathode material was found to be 45 nm thereby leads to the feasible movement of lithium ion all through the material. FT-IR spectroscopy was used to confirm the metal-oxygen interaction in the prepared cathode material. The electrical properties of the Li (Li_0.05Ni_0.6Fe_0.1Mn_0.25)O₂cathode material were studied by impedance and dielectric spectral analyzes. Li (Li_0.05Ni_0.6Fe_0.1Mn_0.25)O₂showed a maximum ionic conductivity of 10^-6S/cm at ambient temperature.

Keywords:

Sol-gel synthesis, Li(Li_0.05Ni_0.6Fe0.1Mn_0.25)O₂, nanoparticles, lithium ion batteries

1. Introduction

2. Experimental Detams

3. Results and Discussion

4. Conclusions

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Synthesis and Characterization of Li(Li0.05Ni0.6Fe0.1Mn0.25)O2 Cathode Material for Lithim Ion Batteries